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4EDZ

Crystal structure of hH-PGDS with water displacing inhibitor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Detector technologyCCD
DetectorMAR CCD 165 mm
Wavelength(s)1.5418
Spacegroup nameI 41
Unit cell lengths124.468, 124.468, 105.927
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000 - 2.000
R-factor0.1919
Rwork0.190
R-free0.23600
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle0.977
Data scaling softwareSCALEPACK
Phasing softwarePHASER
Refinement softwareREFMAC
Data quality characteristics
 OverallInner shellOuter shell
Low resolution limit [Å]50.00050.0002.070
High resolution limit [Å]2.0004.3102.000
Rmerge0.0950.0690.307
Number of reflections49416
<I/σ(I)>5.8
Completeness [%]90.384.689
Redundancy2.12.52
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSIONvapor diffusion

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PDB entries from 2024-09-18

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