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4C9Z

Crystal structure of Siah1 at 1.95 A resolution

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU MICROMAX-007
Temperature [K]287
Detector technologyIMAGE PLATE
Collection date2011-04-12
DetectorRIGAKU RAXIS IV
Spacegroup nameI 2 2 2
Unit cell lengths75.140, 104.590, 133.160
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution40.000 - 1.950
R-factor0.19967
Rwork0.198
R-free0.23855
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)2a25
RMSD bond length0.011
RMSD bond angle1.302
Data reduction softwareiMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.5.0102)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]44.9902.060
High resolution limit [Å]1.9501.950
Rmerge0.0400.180
Number of reflections38340
<I/σ(I)>19.34.5
Completeness [%]99.396
Redundancy3.72.1
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1CRYSTALS GREW FROM EQUAL VOLUMES OF PROTEIN SOLUTION (15 MG ML-1 IN 15 MM TRIS-HCL PH7.5, 30 MM NACL AND 10 MM DTT) AND RESERVOIR SOLUTION (100 MES PH6.5, 1.5 M MGSO4).

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