3RGF
Crystal Structure of human CDK8/CycC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2010-05-10 |
Detector | PSI PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 70.690, 70.610, 79.140 |
Unit cell angles | 90.00, 108.31, 90.00 |
Refinement procedure
Resolution | 37.567 - 2.200 |
R-factor | 0.1826 |
Rwork | 0.180 |
R-free | 0.22090 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ENTRIES 1ZP2 2i53 2pk2 2WH2 2pk2 2rk3 2uze 2r3q 2r3n 2vth |
RMSD bond length | 0.007 |
RMSD bond angle | 1.004 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | BALBES |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.567 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.089 | 0.542 |
Number of reflections | 37725 | |
<I/σ(I)> | 10.7 | 2.6 |
Completeness [%] | 100.0 | 99.9 |
Redundancy | 4.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG3350, 0.2M lithium chloride, VAPOR DIFFUSION, HANGING DROP, temperature 293K |