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3REL

2.7 Angstrom Crystal Structure of the Nucleosome Core Particle Assembled with a 146 bp Alpha-Satellite DNA (NCP146b) Derivatized with Triamminechloroplatinum(II) Chloride

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X06SA
Synchrotron siteSLS
BeamlineX06SA
Detector technologyCCD
DetectorMARMOSAIC 225 mm CCD
Wavelength(s)1.07
Spacegroup nameP 21 21 21
Unit cell lengths105.659, 109.697, 175.654
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution59.000 - 2.700
R-factor0.24972
Rwork0.249
R-free0.30162
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1kx4
RMSD bond length0.010
RMSD bond angle1.447
Refinement softwareREFMAC (5.2.0019)
Data quality characteristics
 Overall
Low resolution limit [Å]59.000
High resolution limit [Å]2.700
Rmerge0.075
Number of reflections53327
<I/σ(I)>19.8
Completeness [%]96.4
Redundancy4.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1

217705

PDB entries from 2024-03-27

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