3MJR

Human dCK complex with Acyclic Nucleoside

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2006-04-17
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.54
Spacegroup name	P 41
Unit cell lengths	97.310, 97.310, 121.500
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.100
Rwork	0.258
R-free	0.31200
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	: 2ZI6
RMSD bond length	0.008
RMSD bond angle	1.228
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	REFMAC

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.155
High resolution limit [Å]	2.100	2.100
Number of reflections	65000
<I/σ(I)>		4.2
Completeness [%]	98.4	90.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	285	1M Sodium Citrate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 285K