3KSL

Structure of FPT bound to DATFP-DH-GPP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU FR-E+ SUPERBRIGHT
Temperature [K]	95
Detector technology	IMAGE PLATE
Collection date	2009-04-29
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.5418
Spacegroup name	P 61
Unit cell lengths	171.191, 171.191, 69.217
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	29.450 - 2.050
Rwork	0.180
R-free	0.21450
Structure solution method	FOURIER SYNTHESIS
Starting model (for MR)	1o1t
RMSD bond length	0.010
RMSD bond angle	0.990
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	BUSTER (2.9.2)
Refinement software	BUSTER (2.9.2)

Data quality characteristics

	Overall
Low resolution limit [Å]	29.450
High resolution limit [Å]	2.050
Rmerge	0.061
Number of reflections	71190
<I/σ(I)>	20.3
Completeness [%]	97.9
Redundancy	3.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.7	298	PEG 4000, SODIUM ACETATE, KCL, pH 5.7, VAPOR DIFFUSION, HANGING DROP, temperature 298K