3K23
Glucocorticoid Receptor with Bound D-prolinamide 11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2006-12-15 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 184.927, 65.956, 71.528 |
Unit cell angles | 90.00, 103.64, 90.00 |
Refinement procedure
Resolution | 19.820 - 3.000 |
R-factor | 0.229 |
Rwork | 0.224 |
R-free | 0.28900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | homology model generated from PR LBD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.243 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 3.110 |
High resolution limit [Å] | 3.000 | 6.460 | 3.000 |
Rmerge | 0.079 | 0.037 | 0.381 |
Number of reflections | 16987 | ||
<I/σ(I)> | 8.1 | ||
Completeness [%] | 99.1 | 99 | 93.2 |
Redundancy | 3.6 | 3.5 | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298 | 0.1M MES 6.5, 28% PEG 5K MME, VAPOR DIFFUSION, HANGING DROP, temperature 298K |