2ZEB
Potent, Nonpeptide Inhibitors of Human Mast Cell Tryptase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Detector technology | CCD |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.0 |
Spacegroup name | P 41 |
Unit cell lengths | 82.670, 82.670, 171.565 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 2.500 |
Rwork | 0.172 |
R-free | 0.22500 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.767 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 30.000 |
High resolution limit [Å] | 2.500 |
Number of reflections | 38453 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |