2YPD
Crystal structure of the Jumonji domain of human Jumonji domain containing 1C protein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-10-17 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 45.718, 112.206, 165.173 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 92.820 - 2.100 |
R-factor | 0.21616 |
Rwork | 0.215 |
R-free | 0.23986 |
Structure solution method | SAD |
Starting model (for MR) | NONE |
RMSD bond length | 0.009 |
RMSD bond angle | 1.241 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | autoSHARP |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 92.820 | 2.160 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.150 | 1.040 |
Number of reflections | 50717 | |
<I/σ(I)> | 11.5 | 1.7 |
Completeness [%] | 100.0 | 100 |
Redundancy | 15.6 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 13% PEG3350, 200 MM SODIUM MALONATE |