2X1W
Crystal Structure of VEGF-C in Complex with Domains 2 and 3 of VEGFR2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-05-25 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.750, 123.830, 211.831 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.958 - 2.700 |
R-factor | 0.2297 |
Rwork | 0.227 |
R-free | 0.27980 |
Structure solution method | SIRAS |
Starting model (for MR) | NONE |
RMSD bond length | 0.005 |
RMSD bond angle | 1.004 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELX (CDE IMPLEMENTED IN HKL2MAP) |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 53.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.070 | 0.730 |
Number of reflections | 53953 | |
<I/σ(I)> | 20.1 | 2.8 |
Completeness [%] | 99.6 | 99.5 |
Redundancy | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.2 | 100 MM MES BUFFER, PH 5.0-5.6, 50 MM CSCL AND 28-32 % (W/V) JEFFAMINE 600. |