2VDY
Crystal structure of the reactive loop cleaved Corticosteroid Binding Globulin complexed with Cortisol
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2007-06-10 |
Detector | MARRESEARCH |
Spacegroup name | P 1 |
Unit cell lengths | 38.673, 39.757, 111.586 |
Unit cell angles | 83.09, 85.70, 69.42 |
Refinement procedure
Resolution | 19.430 - 2.300 |
R-factor | 0.213 |
Rwork | 0.210 |
R-free | 0.27100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1qmn |
RMSD bond length | 0.006 |
RMSD bond angle | 0.969 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.3.0037) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.400 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.080 | 0.460 |
Number of reflections | 22575 | |
<I/σ(I)> | 11 | 2.5 |
Completeness [%] | 93.5 | 91.1 |
Redundancy | 2.2 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.4 | 10-20% PEG3350, 0.2M NACL, pH 7.4 |