2I4Q
Human renin/PF02342674 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 170 |
Detector technology | CCD |
Collection date | 2004-06-11 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 3 |
Unit cell lengths | 141.898, 141.898, 141.898 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.000 - 2.300 |
R-factor | 0.23 |
Rwork | 0.229 |
R-free | 0.26100 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.080 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.051 | 0.289 |
Number of reflections | 37838 | |
Completeness [%] | 89.1 | 95.2 |
Redundancy | 2.63 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |