2YPD
Crystal structure of the Jumonji domain of human Jumonji domain containing 1C protein
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2012-10-17 |
| Detector | DECTRIS PILATUS 6M |
| Spacegroup name | P 2 21 21 |
| Unit cell lengths | 45.718, 112.206, 165.173 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 92.820 - 2.100 |
| R-factor | 0.21616 |
| Rwork | 0.215 |
| R-free | 0.23986 |
| Structure solution method | SAD |
| Starting model (for MR) | NONE |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.241 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | autoSHARP |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 92.820 | 2.160 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.150 | 1.040 |
| Number of reflections | 50717 | |
| <I/σ(I)> | 11.5 | 1.7 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 15.6 | 5.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 13% PEG3350, 200 MM SODIUM MALONATE |
