2X1X
CRYSTAL STRUCTURE OF VEGF-C IN COMPLEX WITH DOMAINS 2 AND 3 OF VEGFR2 IN A TETRAGONAL CRYSTAL FORM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2009-04-20 |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 88.733, 88.733, 105.273 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.000 - 3.100 |
R-factor | 0.27292 |
Rwork | 0.266 |
R-free | 0.33391 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2x1w |
RMSD bond length | 0.006 |
RMSD bond angle | 1.114 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0072) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.000 | 3.200 |
High resolution limit [Å] | 3.100 | 3.100 |
Rmerge | 0.100 | 0.550 |
Number of reflections | 8092 | |
<I/σ(I)> | 29.2 | 7.5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 17.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 100 MM NA-ACETATE BUFFER, PH 4.4-4.8, 50 MM CSCL, 28-32 % (W/V) JEFFAMINE 600 |