2I4Q

Human renin/PF02342674 complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	170
Detector technology	CCD
Collection date	2004-06-11
Detector	ADSC QUANTUM 210
Wavelength(s)	1.000
Spacegroup name	P 21 3
Unit cell lengths	141.898, 141.898, 141.898
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	35.000 - 2.300
R-factor	0.23
Rwork	0.229
R-free	0.26100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.080
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	35.000	2.380
High resolution limit [Å]	2.300	2.300
Rmerge	0.051	0.289
Number of reflections	37838
Completeness [%]	89.1	95.2
Redundancy	2.63

Crystallization Conditions

crystal ID	method	pH	temperature	details
1