1UWH
The complex of wild type B-RAF and BAY439006.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID13 |
Synchrotron site | ESRF |
Beamline | ID13 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2003-03-15 |
Detector | MARRESEARCH |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 110.280, 110.280, 143.010 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 3.070 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.123 | 0.351 |
Total number of observations | 66126 * | |
Number of reflections | 18727 | 1968 * |
<I/σ(I)> | 8.8 | 2.1 |
Completeness [%] | 98.0 | 98 |
Redundancy | 3.5 | 2.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 8.5 | 20 * | pH 8.50 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | Tris-HCl | 100 (mM) | pH8.5 |
2 | 1 | 1 | PEG8000 | 8 (%(w/v)) |