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1NY2

Human alpha thrombin inhibited by RPPGF and hirugen

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RU200
Temperature [K]298
Detector technologyIMAGE PLATE
Collection date1997-11-11
DetectorRIGAKU RAXIS II
Wavelength(s)1.5418
Spacegroup nameP 21 21 2
Unit cell lengths79.150, 104.970, 45.180
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution8.000 - 2.300
Rwork0.202
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1dit
RMSD bond length0.020
RMSD bond angle0.047
Phasing softwareAMoRE
Refinement softwarePROLSQ
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.300
High resolution limit [Å]2.1002.100
Rmerge0.068
Number of reflections17158
Completeness [%]73.00.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion

*

4.6298PEG 4000, ammonium sulphate, sodium acetate, pH 4.6, VAPOR DIFFUSION, HANGING DROP, temperature 25K, temperature 298K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirPEG400023.5 (%)
21reservoirsodium acetate0.1 (M)pH4.6
31reservoirammonium sulfate0.2 (M)

225158

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