1C8T
HUMAN STROMELYSIN-1 (E202Q) CATALYTIC DOMAIN COMPLEXED WITH RO-26-2812
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | AREA DETECTOR |
Collection date | 1995-01-01 |
Detector | SDMS |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 120.100, 47.000, 54.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.600 |
R-factor | 0.22 |
RMSD bond length | 0.011 * |
RMSD bond angle | 2.500 * |
Data reduction software | SDMS |
Data scaling software | SDMS |
Phasing software | AMoRE |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
High resolution limit [Å] | 2.150 | 2.150 |
Rmerge | 0.079 | |
Number of reflections | 15629 | |
<I/σ(I)> | 19 | |
Completeness [%] | 88.9 * | |
Redundancy | 5.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 22 * | PEG, potassium chloride, calcium chloride, cacodylate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | mPEG6000 | 100 (mM) | or mPEG8000 |
2 | 1 | reservoir | 50 (mM) | ||
3 | 1 | reservoir | 200 (mM) |