1TSD
THYMIDYLATE SYNTHASE COMPLEX WITH 2'-DEOXYURIDINE 5'-MONOPHOSPHATE (DUMP) AND FOLATE ANALOG 1843U89
Experimental procedure
Detector technology | DIFFRACTOMETER |
Collection date | 1993-06-21 |
Detector | ENRAF-NONIUS FAST |
Spacegroup name | P 63 |
Unit cell lengths | 127.520, 127.520, 68.250 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.000 - 1.950 |
R-factor | 0.197 |
RMSD bond length | 0.020 |
RMSD bond angle | 0.045 |
Data reduction software | MADNES |
Refinement software | GPRLSA |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 |
High resolution limit [Å] | 1.950 |
Rmerge | 0.087 |
Number of reflections | 48550 |
Completeness [%] | 98.0 |
Redundancy | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | E. coli | 31 (mg/ml) | |
2 | 1 | drop | dUMP | 5 (mM) | |
3 | 1 | drop | 1843U89 | 0.5 (mM) | |
4 | 1 | drop | phosphate | 20 (mM) | |
5 | 1 | drop | 2-mercaptoethanol | 20 (mM) | |
6 | 1 | reservoir | ammonium sulfate | 2.6 (M) |