9B7B
Crystal structure of humanized 44H10 Fab Version 22 in complex with HLA-DR (HLA-DRA*01:01/HLA-DRB1*04:01)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-11-01 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.953570 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 169.586, 178.801, 178.359 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.560 - 3.080 |
R-factor | 0.2017 |
Rwork | 0.200 |
R-free | 0.23680 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 0.806 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.600 | 3.360 |
High resolution limit [Å] | 3.080 | 3.080 |
Number of reflections | 29589 | 1974 |
<I/σ(I)> | 7.8 | |
Completeness [%] | 93.0 | |
Redundancy | 13.6 | |
CC(1/2) | 0.977 | 0.470 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 20% (w/v) PEG 6000, 0.1 M citric acid, pH 4.0 |