Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-11-18 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.980000 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 90.627, 90.627, 122.181 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 36.395 - 1.700 |
| R-factor | 0.1465 |
| Rwork | 0.146 |
| R-free | 0.16450 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.248 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 36.400 | 1.761 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.073 | |
| Number of reflections | 63419 | 5673 |
| <I/σ(I)> | 17.99 | |
| Completeness [%] | 98.6 | |
| Redundancy | 8.8 | |
| CC(1/2) | 0.999 | 0.875 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | Sodium acetate (pH 4.8), Ammonium sulfate, Glycerol |
