8XOX
The Crystal Structure of FAK2 from Biortus.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-09-16 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.953732 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.797, 59.132, 67.295 |
| Unit cell angles | 90.00, 95.03, 90.00 |
Refinement procedure
| Resolution | 44.384 - 1.900 |
| Rwork | 0.169 |
| R-free | 0.22980 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.398 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.384 | 1.940 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.084 | 0.701 |
| Number of reflections | 23394 | 1465 |
| <I/σ(I)> | 13.7 | |
| Completeness [%] | 99.8 | |
| Redundancy | 6.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M LiCl2, 0.1M Tris pH8.0, 20% PEG 6000 |
