8VUI
Structure of FabS1CE-EPR-1, an elbow-locked Fab, in complex with the erythropoeitin receptor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-21 |
Detector | DECTRIS EIGER2 X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 56.390, 71.930, 197.020 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 98.510 - 2.100 |
R-factor | 0.1991 |
Rwork | 0.197 |
R-free | 0.23980 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.943 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 98.510 | 2.120 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 0.107 | 1.193 |
Rmeas | 0.117 | 1.298 |
Rpim | 0.046 | 0.506 |
Number of reflections | 46837 | 2699 |
<I/σ(I)> | 9.3 | 1.9 |
Completeness [%] | 92.5 | 69.7 |
Redundancy | 6.5 | 6.6 |
CC(1/2) | 0.995 | 0.723 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.2 | 298 | 0.2 M Ammonium Citrate dibasic, 20% PEG2000 monomethyl ether, pH 5.2 |