8VEU
Crystal structure of PRMT5:MEP50 in complex with MTA and oxamide compound 23
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CLSI BEAMLINE 08ID-1 |
Synchrotron site | CLSI |
Beamline | 08ID-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-25 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97779 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 103.370, 138.790, 179.710 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.800 - 2.460 |
R-factor | 0.2034 |
Rwork | 0.201 |
R-free | 0.25027 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.006 |
RMSD bond angle | 1.483 |
Data reduction software | XDS |
Data scaling software | Aimless |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.800 | 2.550 |
High resolution limit [Å] | 2.460 | 2.460 |
Rmerge | 0.078 | 0.934 |
Rmeas | 0.085 | 1.013 |
Rpim | 0.033 | 0.390 |
Total number of observations | 30741 | |
Number of reflections | 47213 | 4610 |
<I/σ(I)> | 14.5 | 2.2 |
Completeness [%] | 99.9 | |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 0.999 | 0.875 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 291 | 10% PEG 4000, 0.2M magnesium chloride, 0.1M sodium citrate (pH 6.0) |