8TLZ
Preclinical Characterization of Pan-NKG2D Ligand-Binding NKG2D Receptor Decoys
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.1 |
Synchrotron site | ALS |
Beamline | 5.0.1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2016-01-30 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97648 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 127.823, 127.823, 157.017 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 110.700 - 2.750 |
R-factor | 0.23257 |
Rwork | 0.230 |
R-free | 0.26999 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.241 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 110.700 | 50.000 | 2.800 |
High resolution limit [Å] | 2.750 | 7.460 | 2.750 |
Rmerge | 0.077 | 0.026 | 0.752 |
Rmeas | 0.028 | 0.786 | |
Rpim | 0.008 | 0.221 | |
Number of reflections | 20359 | 1155 | 995 |
<I/σ(I)> | 19.5 | ||
Completeness [%] | 99.9 | 98.9 | 100 |
Redundancy | 12.3 | 11.3 | 12.2 |
CC(1/2) | 1.000 | 0.937 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | Peg 3350, DL-Malic acid (pH 7.0) |