8PAU
Crystal structure of MAP4K1 with a SMOL inhibitor
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.99984 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 60.983, 99.904, 61.101 |
Unit cell angles | 90.00, 101.94, 90.00 |
Refinement procedure
Resolution | 47.460 - 2.800 |
R-factor | 0.21928 |
Rwork | 0.217 |
R-free | 0.27230 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.647 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.460 | 3.050 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmeas | 0.063 | 0.511 |
Number of reflections | 17639 | 3972 |
<I/σ(I)> | 20.2 | 3.99 |
Completeness [%] | 99.4 | 99.4 |
Redundancy | 3.3 | 3.3 |
CC(1/2) | 0.999 | 0.927 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | NOT DISCLOSED |