8OS5
Crystal structure of the Factor XII heavy chain reveals an interlocking dimer with a FnII to kringle domain interaction
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 93 |
Detector technology | PIXEL |
Collection date | 2018-12-06 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 144.536, 144.594, 155.935 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 77.970 - 3.400 |
R-factor | 0.2616 |
Rwork | 0.255 |
R-free | 0.31880 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.535 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 77.970 | 3.716 |
High resolution limit [Å] | 3.394 | 3.394 |
Number of reflections | 14002 | 701 |
<I/σ(I)> | 7.1 | |
Completeness [%] | 94.2 | |
Redundancy | 6.4 | |
CC(1/2) | 0.994 | 0.585 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 293 | 5% PAA1200, 0.1M urea. |