8K62
Crystal structure of ALKBH1 and 13h complex.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-08-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 65 |
Unit cell lengths | 56.502, 56.502, 192.135 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 34.278 - 1.991 |
R-factor | 0.2114 |
Rwork | 0.204 |
R-free | 0.27770 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ie2 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.337 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.420 | 2.100 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.101 | 1.600 |
Rmeas | 0.103 | 1.644 |
Rpim | 0.023 | 0.372 |
Total number of observations | 412841 | 44551 |
Number of reflections | 20666 | 2353 |
<I/σ(I)> | 20.5 | 2.4 |
Completeness [%] | 86.9 | |
Redundancy | 20 | 18.9 |
CC(1/2) | 1.000 | 0.938 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 0.1M imidazole, pH7.0, 20% Polyrthylene glycol 6000 |