8JF3
C-Src in complex with compound 9
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CAMD BEAMLINE GCPCC |
Synchrotron site | CAMD |
Beamline | GCPCC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-09 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 |
Unit cell lengths | 41.716, 63.427, 73.649 |
Unit cell angles | 101.21, 91.05, 90.16 |
Refinement procedure
Resolution | 62.215 - 2.846 |
R-factor | 0.278454516745 |
Rwork | 0.274 |
R-free | 0.31693 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.665 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.230 | 2.940 |
High resolution limit [Å] | 2.840 | 2.840 |
Number of reflections | 16792 | 16792 |
<I/σ(I)> | 5.5 | |
Completeness [%] | 96.7 | |
Redundancy | 3.1 | |
CC(1/2) | 0.991 | 0.894 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 300 mM Sodium Acetate, 0.1 M MES pH 7.5, 4% PEG3350 |