8F93
WDR5 covalently modified at Y228 by (R)-2-SF
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 2.0.1 |
Synchrotron site | ALS |
Beamline | 2.0.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 92.780, 103.022, 81.014 |
Unit cell angles | 90.00, 101.55, 90.00 |
Refinement procedure
Resolution | 32.260 - 2.300 |
R-factor | 0.2055 |
Rwork | 0.203 |
R-free | 0.25270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.012 |
RMSD bond angle | 1.236 |
Data reduction software | MOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.260 | 2.382 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.077 | 0.787 |
Number of reflections | 32875 | 3285 |
<I/σ(I)> | 9.2 | |
Completeness [%] | 99.0 | |
Redundancy | 3.3 | |
CC(1/2) | 0.997 | 0.731 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.2 M Ammonium sulfate, 0.1 M MES pH 6.5, 20% w/v PEG 8000 |