8E3G
BMP2/GDF5 heterodimer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2017-04-10 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 98.321, 98.321, 174.783 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 76.600 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.173 | 1.363 |
Rpim | 0.055 | 0.426 |
Number of reflections | 24734 | 2428 |
<I/σ(I)> | 11.2 | 2.3 |
Completeness [%] | 100.0 | |
Redundancy | 11 | 11.2 |
CC(1/2) | 0.995 | 0.709 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | Tris, magnesium formate |