8D7I
Bifunctional Inhibition of Neutrophil Elastase and Cathepsin G by Eap1 from S. aureus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-27 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 102.230, 152.270, 296.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 96.640 | 84.900 | 3.760 |
High resolution limit [Å] | 3.630 | 7.820 | 3.630 |
Rmerge | 0.040 | 0.012 | 0.156 |
Rpim | 0.040 | 0.012 | 0.156 |
Number of reflections | 53125 | 5595 | 5226 |
<I/σ(I)> | 5.1 | 38.9 | 5.1 |
Completeness [%] | 99.9 | 99.7 | 100 |
Redundancy | 2 | 2 | 2 |
CC(1/2) | 0.998 | 0.999 | 0.949 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.9 | 293 | 0.1M BisTris, 0.2M sodium/potassium tartrate, 14% PEG-8000 |