8CGZ
tubulin-AB8939 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-17 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98011 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 65.692, 128.760, 253.204 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 126.600 - 2.527 |
R-factor | 0.1992 |
Rwork | 0.197 |
R-free | 0.23500 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.008 |
RMSD bond angle | 0.900 |
Data reduction software | XDS |
Data scaling software | autoPROC |
Phasing software | BUSTER |
Refinement software | BUSTER (2.10.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 126.600 | 2.760 |
High resolution limit [Å] | 2.530 | 2.530 |
Rmeas | 0.145 | |
Rpim | 0.040 | 0.521 |
Number of reflections | 47709 | 1871 |
<I/σ(I)> | 12.7 | 1.5 |
Completeness [%] | 66.5 | |
Redundancy | 13.1 | 13.1 |
CC(1/2) | 0.996 | 0.354 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293 | PEG, LiSO4, PIPES BUFFER, pH 6.80 |