8CAA
Crystal structure of TEAD4 in complex with YTP-13
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-03 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 35.729, 89.397, 135.473 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.440 - 1.999 |
R-factor | 0.2138 |
Rwork | 0.213 |
R-free | 0.23730 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.010 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | BUSTER (2.11.8 (8-JUN-2022)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.440 | 2.090 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.135 | 1.323 |
Rmeas | 0.151 | 1.436 |
Number of reflections | 26699 | 1335 |
<I/σ(I)> | 9.6 | 1.7 |
Completeness [%] | 88.2 | 35.7 |
Redundancy | 6.6 | 6.7 |
CC(1/2) | 0.998 | 0.584 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 22% PEG 3350 (w/v) , 0.25 M ammonium citrate dibasic |