8C0F
Tubulin-PTC596 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-14 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 0.999995 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.680, 158.260, 180.540 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.550 - 2.100 |
R-factor | 0.1956 |
Rwork | 0.194 |
R-free | 0.22520 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 5lxt |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX (1.15.2_3472) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.550 | 49.550 | 2.160 |
High resolution limit [Å] | 2.100 | 9.390 | 2.100 |
Rmerge | 0.138 | 0.019 | 3.965 |
Rmeas | 0.144 | 0.019 | 4.122 |
Total number of observations | 2378365 | ||
Number of reflections | 174197 | 2135 | 12635 |
<I/σ(I)> | 15.97 | 101.29 | 0.7 |
Completeness [%] | 99.7 | 98.6 | 98.6 |
Redundancy | 13.653 | 12.572 | 13.28 |
CC(1/2) | 0.999 | 1.000 | 0.259 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293 | 3% PEG 4K, 3% glycerol, 30 mM MgCl2, 30 mM CaCl2, 0.1 M MES/Imidazole, 5 mM L-tyrosine |