8YX1
CD40 in complex with Bleselumab Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-12-20 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 49.565, 116.002, 121.651 |
Unit cell angles | 90.00, 91.71, 90.00 |
Refinement procedure
Resolution | 45.560 - 2.700 |
Rwork | 0.204 |
R-free | 0.26510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.560 |
Data reduction software | XDS (20210323) |
Data scaling software | Aimless (0.7.4) |
Phasing software | PHASER (2.8.3) |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.560 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.143 | 0.941 |
Rpim | 0.059 | 0.537 |
Number of reflections | 37822 | 4604 |
<I/σ(I)> | 12.8 | 2.3 |
Completeness [%] | 99.9 | 100 |
Redundancy | 6.8 | 6.9 |
CC(1/2) | 0.996 | 0.824 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.2 M Ammonium chloride 20% w/v Polyethylene glycol 3,350 |