8R9A
A soakable crystal form of human CDK7 in complex with AMP-PNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-11-20 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99987 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 144.433, 40.417, 68.676 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 72.220 - 1.710 |
R-factor | 0.2236 |
Rwork | 0.220 |
R-free | 0.29390 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.010 |
RMSD bond angle | 1.305 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 72.220 | 1.717 |
High resolution limit [Å] | 1.710 | 1.710 |
Rmeas | 0.173 | 1.232 |
Number of reflections | 18453 | 969 |
<I/σ(I)> | 7.8 | |
Completeness [%] | 85.5 | |
Redundancy | 6.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | .2M Na2HPO4 20% PEG 3350 |