Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-08-21 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 0.99997 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 128.586, 103.948, 191.816 |
| Unit cell angles | 90.00, 100.17, 90.00 |
Refinement procedure
| Resolution | 63.474 - 3.060 |
| Rwork | 0.191 |
| R-free | 0.23520 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.445 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 71.103 | 3.067 |
| High resolution limit [Å] | 3.057 | 3.057 |
| Rmerge | 0.130 | 0.540 |
| Number of reflections | 47077 | 482 |
| <I/σ(I)> | 9.3 | |
| Completeness [%] | 99.6 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 0.1 M Bis-Tris, 0.3 M MgCl2, 20% PEG 3350 |
