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8PYI

Human IGF1R with inhibitor 6

This is a non-PDB format compatible entry.
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSLS BEAMLINE X10SA
Synchrotron siteSLS
BeamlineX10SA
Temperature [K]100
Detector technologyPIXEL
Collection date2014-08-21
DetectorDECTRIS PILATUS 2M
Wavelength(s)0.99997
Spacegroup nameC 1 2 1
Unit cell lengths128.586, 103.948, 191.816
Unit cell angles90.00, 100.17, 90.00
Refinement procedure
Resolution63.474 - 3.060
Rwork0.191
R-free0.23520
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.445
Data reduction softwareXDS
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0267)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]71.1033.067
High resolution limit [Å]3.0573.057
Rmerge0.1300.540
Number of reflections47077482
<I/σ(I)>9.3
Completeness [%]99.6
Redundancy3.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION2930.1 M Bis-Tris, 0.3 M MgCl2, 20% PEG 3350

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