8PJE
Human Leukocyte Antigen class II allotype DR1 presenting influenza A virus haemagglutinin (HA)306-318 PKYVKQNTLKLAT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-13 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97625 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.500, 89.180, 137.440 |
Unit cell angles | 90.00, 90.90, 90.00 |
Refinement procedure
Resolution | 32.810 - 1.700 |
R-factor | 0.1724 |
Rwork | 0.171 |
R-free | 0.20260 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.639 |
Data reduction software | xia2 |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 32.810 | 1.760 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.083 | 0.884 |
Rmeas | 0.097 | 1.039 |
Rpim | 0.049 | 0.539 |
Number of reflections | 109380 | 10898 |
<I/σ(I)> | 9.48 | 1.36 |
Completeness [%] | 99.5 | 99.55 |
Redundancy | 3.7 | 3.6 |
CC(1/2) | 0.997 | 0.545 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 291 | 0.1 M HEPES pH 7.0, 25 % PEG8000, 15 % Glycerol |