8PAU
Crystal structure of MAP4K1 with a SMOL inhibitor
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-07-01 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.99984 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 60.983, 99.904, 61.101 |
| Unit cell angles | 90.00, 101.94, 90.00 |
Refinement procedure
| Resolution | 47.460 - 2.800 |
| R-factor | 0.21928 |
| Rwork | 0.217 |
| R-free | 0.27230 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.647 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.460 | 3.050 |
| High resolution limit [Å] | 2.800 | 2.800 |
| Rmeas | 0.063 | 0.511 |
| Number of reflections | 17639 | 3972 |
| <I/σ(I)> | 20.2 | 3.99 |
| Completeness [%] | 99.4 | 99.4 |
| Redundancy | 3.3 | 3.3 |
| CC(1/2) | 0.999 | 0.927 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | NOT DISCLOSED |
