8EV1
Dual Modulators
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-BM |
Synchrotron site | APS |
Beamline | 22-BM |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2019-07-18 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 54.055, 82.633, 58.553 |
Unit cell angles | 90.00, 110.93, 90.00 |
Refinement procedure
Resolution | 50.540 - 1.830 |
R-factor | 0.1785 |
Rwork | 0.176 |
R-free | 0.22420 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2qzo |
RMSD bond length | 0.007 |
RMSD bond angle | 1.122 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0253) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.540 | 2.068 |
High resolution limit [Å] | 1.828 | 1.828 |
Rmerge | 0.123 | |
Number of reflections | 27680 | 1385 |
<I/σ(I)> | 12 | |
Completeness [%] | 92.6 | |
Redundancy | 7.6 | |
CC(1/2) | 0.998 | 0.513 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 298 | 20-25% PEG 3350, 200 mM MgCl2, 200 mM NaCl, 0.1 M Hepes pH 7 |