8CR3
Crystal structure of recombinant LasB from Pseudomonas aeruginosa PAO1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-24 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.68880 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 40.542, 89.875, 41.340 |
Unit cell angles | 90.00, 113.96, 90.00 |
Refinement procedure
Resolution | 28.590 - 1.120 |
R-factor | 0.1622 |
Rwork | 0.162 |
R-free | 0.17010 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.050 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.938 | 1.136 |
High resolution limit [Å] | 1.116 | 1.116 |
Rmerge | 0.071 | 0.565 |
Rmeas | 0.086 | 0.683 |
Rpim | 0.048 | 0.380 |
Number of reflections | 190922 | 5145 |
<I/σ(I)> | 8.9 | |
Completeness [%] | 98.9 | |
Redundancy | 3.1 | |
CC(1/2) | 0.994 | 0.736 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M magnesium formate, 20% (w/v) PEG 3350 |