7ZSC
Crystal structure of the heterodimeric human C-P4H-II with truncated alpha subunit (C-P4H-II delta281)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P14 (MX2) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P14 (MX2) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-09 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9763 |
Spacegroup name | H 3 |
Unit cell lengths | 252.879, 252.879, 89.400 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.690 | 3.990 |
High resolution limit [Å] | 3.850 | 3.850 |
Rmerge | 0.064 | 1.862 |
Rmeas | 0.071 | 2.058 |
Rpim | 0.031 | 0.873 |
Number of reflections | 20176 | 1969 |
<I/σ(I)> | 8.2 | 0.7 |
Completeness [%] | 99.9 | 100 |
Redundancy | 5.3 | 5.5 |
CC(1/2) | 0.996 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6 | 278 | 20% (w/v) PEG4000, 0.2 M lithium sulfate, 0.1 M MES, 3% methanol |