Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

7XTX

High resolution crystal structure of human macrophage migration inhibitory factor in complex with methotrexate

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron sitePhoton Factory
BeamlineAR-NW12A
Temperature [K]100
Detector technologyCCD
Collection date2017-12-02
DetectorADSC QUANTUM 270
Wavelength(s)1
Spacegroup nameP 21 21 21
Unit cell lengths67.520, 68.284, 88.477
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution34.140 - 1.280
R-factor0.1709
Rwork0.170
R-free0.18800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)5j7q
RMSD bond length0.005
RMSD bond angle0.801
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwarePHENIX (1.16_3549)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.330
High resolution limit [Å]1.2801.280
Number of reflections10419410126
<I/σ(I)>27.4
Completeness [%]98.396.7
Redundancy6.7
CC(1/2)1.0000.730
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP82832.0 M Ammonium sulfate 0.1 M Tris-HCl (pH 8.0) 4 % isopropanol

221051

PDB entries from 2024-06-12

PDB statisticsPDBj update infoContact PDBjnumon