7WVK
Crystal structure of human WDR5 in complex with compound 19
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-01-26 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97915 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 78.330, 98.380, 79.806 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 41.870 - 1.420 |
R-factor | 0.1639 |
Rwork | 0.163 |
R-free | 0.18240 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4y7r |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.18.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.870 | 1.421 |
High resolution limit [Å] | 1.416 | 1.416 |
Number of reflections | 58768 | |
<I/σ(I)> | 18.9 | |
Completeness [%] | 99.9 | |
Redundancy | 8.2 | |
CC(1/2) | 0.999 | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 291 | 0.1M Bis-Tris, 0.2 M NH4OAC, 30% PEG3350 |