7WJQ
Crystal structure of GSDMB in complex with Ipah7.8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-10-06 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 70.471, 87.584, 102.794 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.430 - 2.700 |
R-factor | 0.2123 |
Rwork | 0.210 |
R-free | 0.25220 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5tj4 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.542 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.670 | 2.830 |
High resolution limit [Å] | 2.700 | 2.700 |
Rmerge | 0.077 | |
Number of reflections | 17543 | 2254 |
<I/σ(I)> | 22.6 | |
Completeness [%] | 97.0 | |
Redundancy | 10.7 | |
CC(1/2) | 0.999 | 0.967 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | LIQUID DIFFUSION | 291.15 | NaCl, HEPES sodium, PEG 8000, ammonium sulfate, 1,6-hexanediol |