7VKE
Crystal structure of human CD38 ECD in complex with UniDab(TM) F11A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-08 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 64.820, 64.820, 201.316 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.080 | 1.830 |
High resolution limit [Å] | 1.790 | 1.790 |
Rmerge | 0.083 | 1.379 |
Number of reflections | 47342 | 2686 |
<I/σ(I)> | 12.1 | |
Completeness [%] | 100.0 | |
Redundancy | 10.1 | |
CC(1/2) | 0.999 | 0.653 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Sodium Citrate, PEG 8000 |