7S7I
Crystal structure of Fab in complex with MICA alpha3 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-27 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 92.778, 170.432, 148.894 |
Unit cell angles | 90.00, 105.81, 90.00 |
Refinement procedure
Resolution | 44.630 - 2.400 |
R-factor | 0.2222 |
Rwork | 0.220 |
R-free | 0.25950 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5xj4 4nm4 1hyr |
RMSD bond length | 0.010 |
RMSD bond angle | 1.602 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 170.430 | 2.440 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.087 | 0.734 |
Rpim | 0.055 | 0.478 |
Number of reflections | 172438 | 7781 |
<I/σ(I)> | 8.9 | 1.5 |
Completeness [%] | 99.4 | |
Redundancy | 3.5 | |
CC(1/2) | 0.996 | 0.653 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 10% PEG 20000, 0.1 M Na citrate pH 5.4, 0.2 M MgCl2 |