7RLE
Crystal structure of PPAR gamma in complex with CREB-binding protein and agonist GW1929
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-07-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 59.890, 99.422, 109.179 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.710 - 2.500 |
R-factor | 0.2353 |
Rwork | 0.232 |
R-free | 0.27490 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6d94 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.208 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.710 | 2.589 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.134 | 0.534 |
Rmeas | 0.140 | 0.577 |
Rpim | 0.040 | 0.208 |
Number of reflections | 22792 | 2104 |
<I/σ(I)> | 13.49 | 2.06 |
Completeness [%] | 98.2 | 93.02 |
Redundancy | 11.6 | 6.6 |
CC(1/2) | 0.997 | 0.737 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 293.15 | 1M sodium citrate tribasic dihydrate, 0.1M sodium cacodylate, pH 6.5 |