7NUD
Crystal structure of mouse PRMT6 in complex with inhibitor EML734
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-X |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-03-30 |
Detector | DECTRIS PILATUS 300K |
Wavelength(s) | 1.54178 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 41.766, 118.147, 71.998 |
Unit cell angles | 90.00, 104.32, 90.00 |
Refinement procedure
Resolution | 39.500 - 1.650 |
R-factor | 0.1977 |
Rwork | 0.197 |
R-free | 0.21390 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4c03 |
Data reduction software | XDS |
Data scaling software | Aimless (0.7.3) |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.080 | 1.680 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmerge | 0.120 | 2.058 |
Rmeas | 0.123 | 2.215 |
Rpim | 0.028 | 0.802 |
Number of reflections | 81095 | 4071 |
<I/σ(I)> | 14.9 | 1.1 |
Completeness [%] | 99.6 | 99.8 |
Redundancy | 18.5 | 7.3 |
CC(1/2) | 0.999 | 0.479 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 298 | PEG 3,350 20%, NaNO3 200 mM, Tris-HCl pH 7.5 100 mM |